Quality control methods for
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D -Xylose R. C 5 H 10 O 5 . Description. A white, crystalline powder. Specific optical rotation. Dissolve 1g in 10 ml of water; [ ] C 20 D α ° = about +20°. A suitable commercially available reagent. Yeast extract, water-soluble, R. A suitable commercially available reagent. Zinc R, Zn; granulate, powder, or dust. A suitable commercially available reagent. Zinc, AsR, granulated. Granulated zinc R that complies with the following tests: Limit of arsenic. Add 10ml of stannated hydrochloric acid (∼250g/l) AsTS to 50ml of water, and apply the general test for arsenic; use 10 g of granulated zinc R and allow the reaction to continue for 1 hour; no visible stain is produced. Test for sensitivity. Repeat the test for arsenic with the addition of 0.1 ml of dilute arsenic AsTS; a faint, but distinct yellow stain is produced. Zinc acetate R. C 4 H 6 O 4 Zn,2H 2 O. A suitable commercially available reagent. Zinc acetate/aluminium chloride TS. Quality control methods for medicinal plant materials Procedure. Dissolve 200g of zinc acetate R and 5g of aluminium chloride R in sufficient water to produce 1000 ml. Zinc chloride R. ZnCl 2 . A suitable commercially available reagent. Zinc chloride, iodinated, TS. Procedure. Dissolve 40 g of zinc chloride R and 13 g of potassium iodide R in 21 ml of water. Add 1g of iodine R and shake for 15 minutes. Filter if necessary. Storage. Store protected from light. |
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