Study of bentonite-sorbent isotherm
Figure - 4. At 50°C, PH=2.0 on the PEG-400 template (a) and pH=10.2 on SF ni on ni (b), the image of the
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Figure - 4. At 50°C, PH=2.0 on the PEG-400 template (a) and pH=10.2 on SF ni on ni (b), the image of the surface of sorbents with applied loads is ЮКЦ-1 It can be seen from the image that the sorbent pores obtained in the presence of templant PEG- 400 are evenly distributed over the surface and have the same dimensions, while the surface of the sorbents obtained in the presence of GMDA consists of nanoparticles with a monodisperse spherical morphology. Figure 6. Values obtained from the sorption of benzene vapors in mesogovacs 𝑝/𝑝𝑠/(Г(1−𝑝/𝑝𝑠)) = f(p/ps) correspondence to the linear equation Bet based on the graph f(p/ps). In adsorbents obtained in alkaline media, it was observed that the porosity size was 2.25 times smaller than in a porous sorbent obtained in acidic media, while the surface surface comparable to the aging surface was 1.15 times larger. The compatibility of isotherms obtained as a result of adsorption of benzene vapors at different relative pressures with the linear form of the BET equation was studied. 𝑝/𝑝 𝑠 /(Г(1 − 𝑝/𝑝 𝑠 )) = 1/Г 𝑚 ∙ 𝐶 + 𝐶 – 1/Г 𝑚 ∙ 𝐶 ∙ (𝑝/𝑝 𝑠 ) Using different relative pressure (p/ps), the sorbed amount of adsorbate 𝑝/𝑝𝑠/(Г(1−𝑝/𝑝𝑠)) = f(p/ps) graph f(p/ps) has been drawn up (Fig.6). The figures show that the sorbent samples taken at 50 °C correspond to the linear form of the beta model of the benzene vapor adsorption Isotherms at different relative pressures.Calculations were performed on the basis of the adsorbed amount of benzene within the relative pressure p/ps=0.2÷0.8 . It was found that the isotherm of the sorbent 3125 NEUROQUANTOLOGY | OCTOBER 2022 | VOLUME 20 | ISSUE 12 |PAGE 3120-3130| DOI: 10.14704/NQ.2022.20.12.NQ77313 Jamshed Madjidovich Kurbonov et al / STUDY OF BENTONITE-SORBENT ISOTHERM 7 eISSN1303-5150 www.neuroquantology.com sample obtained at pH = 2.0 has a degree of compatibility R 2 = 98.12, and in the sorbent obtained in an alkaline medium - 92.7%, which corresponds to the isotherm model. Also, based on the data obtained as a result of the experiment, sorbents were determined by saturation adsorption volumes (Vs), microgravity volume (W0), mesogravity volume (Wmez) and saturation volume (Vs) by benzene vapor (Table 3). Download 0.94 Mb. Do'stlaringiz bilan baham: |
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