Quality control methods for


Sodium citrate (36.5 g/l) TS


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Sodium citrate (36.5 g/l) TS. A solution of sodium citrate R containing about 
36.5 g of C
6
H
5
Na
3
O
7
per litre. 
Sodium deoxycholate R. C
23
H
39
NaO
4
. Containing not less than 90% of 
C
23
H
39
NaO
4
.
A suitable commercially available reagent. 
Sodium hydroxide R. NaOH. 
A suitable commercially available reagent. 
Sodium hydroxide (240 g/l) TS. A solution of sodium hydroxide R containing 
about 240g of NaOH per litre of carbon-dioxide-free water R. 
 
Sodium hydroxide (80 g/l) TS. A solution of sodium hydroxide R containing 
about 80g of NaOH per litre (approximately 2mol/l). 


Quality control methods for medicinal plant materials 
Sodium hydroxide (1 mol/l) VS. Sodium hydroxide R dissolved in water to 
produce a solution containing 40.01g of NaOH in 1000 ml. 
Method of standardization. Ascertain the exact concentration of the 1 mol/l 
solution in the following manner: Dry about 5g of potassium hydrogen 
phthalate R at 105°C for 3 hours and weigh accurately. If the potassium 
hydrogen phthalate is in the form of large crystals, they should be crushed 
before drying. Dissolve in 75ml of carbon-dioxide-free water R and titrate with 
the sodium hydroxide solution, using phenolphthalein/ethanol TS as indicator. 
Each 0.2042g of potassium hydrogen phthalate is equivalent to 1 ml of sodium 
hydroxide (1 mol/l) VS. Standard solutions of sodium hydroxide should be 
restandardized frequently. 
Storage. Solutions of alkali hydroxides absorb carbon dioxide when exposed to 
air. They should therefore be stored in bottles with suitable non-glass, tightly-
fitting stoppers, provided with a tube filled with soda lime R. 

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