Quality control methods for medicinal plant materials
Chromic acid TS.
Procedure. Dissolve 84g of chromium trioxide R in 700
ml of water and add
slowly, with stirring, 400ml of sulfuric acid (∼1760g/l) TS.
Chromium trioxide R. CrO
3
.
A suitable commercially available reagent.
Copper(11) sulfate R. CuSO
4
,5H
2
O.
A suitable commercially available reagent.
Crystal violet R. C
25
H
30
ClN
3
.
A suitable commercially available reagent.
Cuoxam TS. Tetramine
copper dihydroxide, Schweizer's reagent.
Procedure. Dissolve 10g of copper(II) sulfate R in 100 ml of water, and add
sufficient sodium hydroxide (∼240g/l) TS until alkaline. Filter the precipitate
and
wash with cold water, previously made sulfate-free. To the moist copper
hydroxide add,
while stirring, ammonia (∼100g/l) TS until dissolved.
Note. Cuoxam TS must be freshly prepared.
Cyclohexane R. C
6
H
12
.
A suitable commercially available reagent.
Desmetryn R. C
9
H
17
N
5
S; 2-methylmercapto-4-methylamino-6-isopropylamino-
S-triazine.
A commercially available reagent suitable for use as a reference material.
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