Quality control methods for medicinal plant materials
Methyl orange R. Sodium salt of 4'-dimethylaminoazobenzene-4-sulfonic acid,
C
14
H
14
N
3
NaO
3
S.
A suitable commercially available reagent.
Methyl orange/ethanol TS.
Procedure. Dissolve 0.04g of methyl orange R in sufficient ethanol (∼1508/l) TS to
produce 100ml.
Methyl palmitate R. Methyl hexadecanoate; C
17
H
34
O
2
.
Description. A
colourless, waxy solid.
Freezing point. About 27°C.
Mass density (ρ
20
). About 0.86kg/l.
A suitable commercially available reagent.
Methyl stearate R. C
19
H
38
O
2
.
Description. A
white or pale yellow, crystalline mass.
Melting point. About 38°C.
A suitable commercially available reagent.
1-Naphthol R. C
10
H
8
O.
Description.
Colourless crystals or a white,
crystalline powder; odour,
characteristic.
Solubility. Soluble in 5 parts of ethanol (∼750 g/l) TS (may
form a slightly
opalescent, colourless or almost colourless solution).
Melting range. 93-96°C.
Sulfated ash. Not more than 0.5 mg/g.
A suitable commercially available reagent.
1-Naphthol TS.
Procedure. Dissolve 20g of 1-naphthol R in 100ml of ethanol (∼750g/l) TS.
Protect
from light and use within a few days of preparation.
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