Nuraliyeva G. A
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Jadval 3. [Cu (BTCK) 2 (MEA) 2] ning asosiy kristallografik ma'lumotlari
h,k,l guruh 0,036 R1, wR2(I>2s (I)) 4,84(9) Qiymatlar 538.03 P-1 m(CuKa), mm-1 X= Cl- , Rint 1199,80(5) ÿ2s (F 0,033, 0,096, 1,06 Kristal o'lchami, mm 0,36 x0,22x0,12 -9:9; -15:15; -17:18 12.42(5) 1.75 0,031 CH3COO Interval Fazoviy 2444 L M = Co(II), Ni(II), Cu(II) va Zn(II). (C2H7NO)2] massa 1.514 L ML2 ni o'z ichiga olgan kompleks birikmalar tuzilishi bilan ifodalangan [Cu(BTSK)2(MEA)2] Sinishi indeksi 105,823(3) 173 Z F 0,63 a, Å b, Å c, Å 1-4 L th,° Singoniya 8833 parametr L Qiymatlar Molekulyar Dx, g/sm V, Å ·· M: L 1: 2 nisbatda etanol eritmasida metallar tuzlari bilan. Refleks 20,69(5) 2444 L Parametr 3 3 4 Rint, 3 1-4 -3 3 1 3 2 4 3 2 2 [Cu(C8H6N3O2)2 4 8 Alieva G.K. _ Machine Translated by Google Mualliflik huquqi © 2021 Muallif(lar). Scientific & Academic Publishing tomonidan nashr etilgan Bu ish Creative Commons Attribution International License (CC BY) ostida litsenziyalangan. http://creativecommons.org/licenses/by/4.0/ [2] Gabbott P. (ed) Termal tahlil tamoyillari va qo'llanilishi. Singapur, Wiley-Blackwell, 2008. 480 p. [13] Sheldrik, GM (2008). Acta Cryst. A64, 112–122. [17] Qu Y., Liu Z.-D., Chju X.-L., Tan M.-Y. Hexaaquanickel (II) bis (p-nitrobenzoat) dihidrat // Acta Crystallogr. -2004.- [8] Jigar EB Noorganik birikmalarning elektron spektroskopiyasi: Per. s burchak. - M .: Mir, 1987. -T.2. -. 443 c. [1] Alieva G.K. Trans-bis (monoetanolamin) bis (2-1 (H-benzotriazol-1- il) sirka kislotasi) mis (II) Acta Crystning tuzilishi. 2019. 2019. E 75. 233-236. [6] Zaikin VGOsnovy organik birikmalarning massa-spektrometriyasi // M .: MAIK "Nauka / Interperiodika", 2001. - [18] Oksford diffraksiyasi (2009). CrysAlis PRO. Oxford Diffraction Ltd, Yarnton, Angliya. 528 c. ISBN 978-5-94836-220-5. [10] Tarasevich BN. Organik birikmalarning asosiy sinflarining IQ spektrlari. Spravochnye materiallari. Moskva. -2012 yil. 55 c. [3] Topor ND, Ogorodova LP, Melchakova LV Minerallar va noorganik birikmalarning termal tahlili. - M .: Izd-vo MGU, 1987. -190 b. [20] Ibragimov A.B., Englert U., Ashurov J.M., Vang A. Materiallar va kimyo xalqaro jurnali 2021, 11(1): 1-9 [14] Yu, KL, Chjan, Y., Civiello, RL, Kadow, KF, Cianci, C., Krystal, M. &. [16] Giordano va Zagari (1978). J. Chem. Soc. Perkin Trans. 2, bet. Str. Kimyo. Matbuotda, 2018 yil. 312–315. [7] Jigar EB Noorganik birikmalarning elektron spektroskopiyasi: Per. s burchak. - M .: Mir, 1987. -T.1.-491 c. [12] Nakamoto K. IK - noorganik va koordinatsion birikmalar spektrlari. M .: Mir. 1996. 204 b. [9] Byokker Yu. Spektroskopiya. Moskva: Texnosfera, 2009 yil. E60. P. m1306-m1307. [5] VA Vinarskiy, RA Yurchenko. Mass-spektrometriya va xromato- massa spektral tahlili: / http://elib.bsu.by/handle/ 123456789/91988. posobie [11] Kazitsina LA, Kupletskaya NB Organik kimyoda UF-, IK va YaMR-spektroskopiyani qo'llash. M.: Kniga po Trebovaniyu. -2013 yil. -264 p. [4] Hokelek T., Necefoglu H. [triaqua (salitsilat) (nikotinamid) sink (II) ning kristall tuzilishi] Analitik fanlar, 2001, jild. 17, yo'q. 10, 1241-1142-betlar. [19] G. Alieva, J. Ashurov, N. Muxamedov. N. Parpiev. 2- (2H- benzotriazol-2-il) sirka kislotasining yangi polimorfi / // Acta Cryst. -2012 yil. -E68. 2833. [15] Meanwell, NA (2003). Bioorg. Med. Kimyo. Lett. 13, 2141–2144. 9 286 b. Hexaaquanikel (II) bis (p-nitrobenzoat) dihidrat tuzining dimorfizmi: yangi triklinik kristall shakli // J. ADABIYOTLAR Machine Translated by Google Download 0.9 Mb. Do'stlaringiz bilan baham: |
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