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ZnO 2
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- 1. INTRODUCTION
Abstract
Zinc oxide (ZnO) Nanopowders were synthesized by the sol–gel method prepared by mixing a methanol solution and Zinc acetate dehydrate and adding ammonia NH4OH to adjust pH value of solution between 9 and 11, the resulting Nanopowders ZnO form a substrate material for the fabrication of ZnO varistors. Microstructure of ZnO nanoparticles were carried out by x-ray diffraction (XRD) that showed that the zinc oxide nanoparticles exhibited hexagonal wurtzite structure. The average particle size was about 12-30 nm. The topographical information of surface were investigated by Atomic Force Microscope (AFM) that showed a homogeneous distribution of nanoparticles with average size of 22 nm which is in good agreement with XRD results, their size distribution was narrow (Fig.6). The I-V characteristics were obtained at a sintering temperature equal to 1,050 °C using MEGOHMMETER. Keywords:ZnO nanoparticles; Sol-gel method; Crystal structure; electrical properties. * Corresponding author. Tel.: +00-963-932-810820; fax: +0-000-000-0000 . E-mail address:Faceeealepuniv@gmail.com 1. INTRODUCTION Oxides of nano particle size in nanometer range have been paid more attention for their unique properties [1-2]. They are widely used for solar energy conversion, non-linear optics, catalysis, varistors, gas sensors, etc [3-6]. Various techniques for the preparation of ZnO Nanopowders have been applied: sol–gel method, co-precipitation method, thermal decomposition, hydrothermal method, etc [7-10]. Among the different methods, the sol-gel approach appears to be one of the most promising methods to prepare ZnO nanoparticles. Some of the most © 2017 The Authors. Published by Elsevier Ltd. Peer-review under responsibility of the Euro-Mediterranean Institute for Sustainable Development (EUMISD). 566 Khalaf AL ABDULLAH et al. / Energy Procedia 119 (2017) 565–570 2 Khalaf AL ABDULLAH, Sahar AWDE/ Energy Procedia 00 (2017) 000–000 important advantages of the sol–gel method are easiness of the synthesis, low temperature of The final decomposition and control on the chemical composition. These advantages make the sol-gel technique a very attractive preparation method. The aim of this study was to synthesize zinc oxide of low dimension and investigation of morphological and electrical properties. This method has novel features, which are of considerable interest due to its low cost, easy preparation and industrial viability. Synthesis of ZnO nanoparticles by a modified sol gel technique is reported by Zinc acetate dehydrate Zn (CH 3 COO) 2 . 2H 2 O precursor and calcined at 500 Co. The structural and electrical properties of ZnO have been studied by XRD, AFM, and MEGOHMMETER-M1500P. Download 119.6 Kb. Do'stlaringiz bilan baham: |
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